Gadolinium and iron based) Deux conditions de synthse sont possibles : Synthse N 1 :Two synthesis conditions are possible: Synthesis N 1: 0,028 g (0,5 mmol) de poudre de Fer mtallique0.028 g (0.5 mmol) of metallic iron powder Fe (Riedel de Han, 99 %), 0,225 g de nitrate de gadolinium(III) hexahydrate (0,5 mmol, Aldrich, 99,9Fe (Riedel de Han, 99%), 0.225 g gadolinium (III) nitrate hexahydrate (0.5 mmol, Aldrich, 99.9%) %), 0,140 g d'acide 1,3,5 benzenetricarboxylique (0,666 mmol, Aldrich 95 %) disperss dans 10 ml d'eau dionise, le tout laiss 24 heures 180 0 C dans un corps en Tflon de 23 ml mis dans une Bombe mtallique PAAR
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Electric heating coil poles are connected to the corresponding power supply anode and cathode